| 曾祥华,余焓,余菁,张俊勇,谢景力.化学通报,2014,77(10):942-950. |
| 连续流动化学方法在无机制备科学中的应用 |
| Application of Continuous Flow Chemistry in Inorganic Synthetic Chemistry |
| 投稿时间：2014-01-12 修订日期：2014-02-03 |
| DOI： |
| 中文关键词: 连续流动化学 微反应器 无机合成 分离和提取 功能材料 |
| 英文关键词:continuous flow chemistry microreactor inorganic synthesis separation and extraction functional materials |
| 基金项目:(No. 21371078)资助 |
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| 中文摘要: |
| “连续流动化学”方法是无机制备科学中一种极具发展潜力的科学手段, 作为一种已发展成熟的过程强化技术,与溶液合成、水热(溶剂热、离子热)等合成方法相比,“连续流动化学”方法具有可精确调控反应速度、缩短反应周期、优化并放大化学反应、提高产率的独特优势。本文总结了当前连续流动化学在无机物的分离和提取,纳米粒子、多金属氧酸盐等无机材料合成等领域的应用,分析了其在无机制备科学中存在的问题并展望了该科学手段的发展趋势。 |
| 英文摘要: |
| Uncovering the unique characters of continuous flow chemistry are the stepping stones to harnessing its power for technological innovation in inorganic synthetic chemistry. Compared to the traditional inorganic synthesis under ‘one-pot’ solution processing conditions and hydrothermal (solvothermal, ionthermal) reaction, continuous flow chemistry is a process intensificaton technology and has its advantage to preciously control reaction rate, speed up and scale up the synthesis, deliver products with better yields etc. This review summarize the application of continuous flow chemistry in separation and extraction of inorganic compounds, synthesis of nanoparticles and polyoxometalates etc. Furthermore, the pros and cos of this technology is briefly discussed. |
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