| 孙敏青,屈凤波,陈鹏丽,王朝杰,杨瑞娜.化学通报,2016,79(11):1093-1096. |
| N,N’-二苯基-N,N’-二(9,9-二甲基芴-2-基)-9-己基-(4,4’-二胺基苯基)咔唑的合成方法及表征 |
| Synthesis and Characterization of N, N |
| 投稿时间：2016-03-11 修订日期：2016-05-23 |
| DOI： |
| 中文关键词: 空穴传输材料 合成 表征 |
| 英文关键词:Hole transport material, Synthesis, Characterization |
| 基金项目: |
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| 中文摘要: |
| 以2,7-二溴咔唑为原料经过N-烷基化、Suzuki偶联反应、Buchwald-Hartwig偶联反应合成了有机发光二极管(OLED)空穴传输材料N,N’-二苯基-N,N’-二(9,9-二甲基芴-2-基)-9-己基-(4,4’-二胺基苯基)咔唑,利用NMR、IR和熔点等分析方法对产物结构进行了表征,并通过TG、UV-Vis及荧光光谱研究了物质的热稳定性和光学性能。 |
| 英文摘要: |
| N, N"- diphenyl - N, N"- bis (9,9-dimethyl-fluoren-2-yl) -9-hexyl group - (4,4"-diamino-phenyl) carbazole as organic light emitting display hole-transport materials was synthesized by N- alkylation, Suzuki coupling reaction, Buchwald-Hartwig coupling reaction using 2,7-dibromo carbazole as starting materials. The structure of target compound was characterized by NMR,IR and melting point. Thermal properties and optical properties were determined with TG, UV-Vis and fluorescence spectrum. |
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