| 王阳,王巧纯.化学通报,2018,81(4):376-379. |
| 基于K2S2O8-KOH体系合成羟基葫芦[6]脲的研究 |
| Investigation of synthesis of Perhydroxycucurbi[6]turil Based on the System Involving K2S2O8-KOH |
| 投稿时间：2017-11-21 修订日期：2017-12-26 |
| DOI： |
| 中文关键词: 羟基葫芦[6]脲 过硫酸钾 氢氧化钾 合成 |
| 英文关键词:perhydroxycucurbi[6]turils KPS KOH synthesis |
| 基金项目:国家自然科学基金项目（21572063；21372076） |
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| 摘要点击次数: 2027 |
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| 中文摘要: |
| 基于已报道的以葫芦脲-过硫酸钾体系的羟基葫芦脲合成反应,我们研究了加入氢氧化钾对原体系的影响,并成功直接得到了目标产物,及较理想的产率27 %。产物由1 H NMR ,13 C NMR和 HR-ESI-MS 所鉴定。 |
| 英文摘要: |
| Based on the reported method using cucurbiturils-potassium peroxydisulfate, the effect of the extra addition of KOH on the synthesis of perhydroxycucurbi[6]turils was investigated,the desired product and adequate yield of 27 % was obtained. The product was further identified by the 1 H NMR, 13 C NMR and HR-ESI-MS. |
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