| 郝勇静,刘欲文,刘海燕.化学通报,2019,82(12):1138-1140. |
| 钼酸铵溶液配制方法的探讨及优化 |
| Discussion and Improvement of Making up Molybdic Acid Ammonium Solution |
| 投稿时间：2019-07-01 修订日期：2019-08-30 |
| DOI： |
| 中文关键词: 钼酸铵溶液 磷酸根 配制 离子鉴定 |
| 英文关键词:Molybdic acid ammonium, Phosphate, Preparing, Ion identification |
| 基金项目:国家自然科学基金项目（21773175）和武汉大学实验教学中心开放实验项目（WHU-2018-XYKF-10） |
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| 中文摘要: |
| 本文针对无机化学实验中钼酸铵溶液的配制方法及使用过程中存在的问题进行了理论分析与实验探究，提出了一种简便可行的钼酸铵溶液配制方法。磷酸根离子鉴定实验结果表明，新方法所配制的钼酸铵溶液检验现象明显且无干扰，在教学实践中取得了理想的效果。该溶液放置一定时间后，检验磷酸根现象与之前无异，便于实验室长期储备。 |
| 英文摘要: |
| In this article, we made a theoretical analysis and experimental study to the problems of preparing molybdic acid ammonium solution in inorganic chemistry teaching experiment. To solve these problems, we present a simple and feasible method for preparing molybdic acid ammonium solution. Ion identification experiment results showed that molybdic acid ammonium solution prepared by our method was sensitive to phosphate ion. The whole process was specific to phosphate ion, and we achieved satisfied experimental result in the teaching experiment. After storing the molybdic acid ammonium solution prepared by our method for 1 year, the ion identification experiment showed similar result for phosphate ion identification, solving the short shelf-time problem of molybdic acid ammonium solution in the inorganic chemistry teaching experiment. |
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