| 刘维,徐奕琳,陈梓莹,倪春林.化学通报,2022,85(4):505-511. |
| 具有荧光和抗菌双重功能的苦味酸吡啶季铵盐的制备综合实验 |
| Comprehensive Experiment on Synthesis of Pyridine Quaternary Ammonium Salt Picric Acid with Fluorescent and Antibacterial Dual Functions |
| 投稿时间：2021-08-03 修订日期：2021-08-18 |
| DOI： |
| 中文关键词: 苦味酸季铵盐 固态荧光 抗菌 综合实验 能力培养 |
| 英文关键词:Picric acid quaternary ammonium salt Fluorescence in solid state Antibacterial properties Comprehensive experiment Ability cultivation |
| 基金项目: |
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| 摘要点击次数: 498 |
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| 中文摘要: |
| 介绍了一项涉及苦味酸吡啶季铵盐制备与性能研究的综合性实验。以吡啶、苦味酸、4-溴苄基溴和碳酸钾等为原料,合成了苦味酸-4-溴苄基吡啶季铵盐([4BrBzPy][PIC]),利用红外光谱、紫外-可见光谱、电喷雾质谱、粉末X-射线衍射和单晶X-射线衍射技术进行了表征,并对其固态荧光和抗菌性能进行研究。该实验项目来源于科研,涵盖多个学科的知识点和实验操作技术,具有综合性和研究性,有利于增强学生勇于探索的创新精神, 培养学生能解决实际问题的能力。适用于应用化学、材料化学、材料科学与工程和制药工程等本科专业综合实验教学。 |
| 英文摘要: |
| A comprehensive experiment on the preparation and properties of pyridine quaternary ammonium salt picric was introduced. 4-Bromobenzyl pyridine quaternary ammonium salt picric acid ([4BrBzPy][PIC]) is synthesized by using 4-bromobenzyl bromide, pyridine, picric acid and potassium carbonate as raw materials. It has been characterized by IR spectrum, UV-Vis spectrum, electrospray mass spectrometry, powder X-ray diffraction and single crystal X-ray diffraction. The fluorescent properties in solid state and antibacterial properties of the salt is investigated. The experiment project covers the multi-disciplinary knowledge and experiment operation technology, and has the characteristics of comprehensiveness and research. The project helps students to cultivate their comprehensive experimental ability and creative ability, and is suitable for undergraduate majors such as applied chemistry, material chemistry and materials science and engineering as comprehensive experiment project. |
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