谭新刚,施小新.化学通报,2022,85(6):755-758. |
育亨宾类似物Sempervilam的全合成 |
The total synthesis of yohimbane analogue Sempervilam |
投稿时间:2021-08-31 修订日期:2021-09-30 |
DOI: |
中文关键词: 育亨宾类似物 合成 |
英文关键词:yohimbane analogue Sempervilam synthesis |
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中文摘要: |
以庚二酸为起始原料,经过十步反应,得到目标产物Sempervilam,总收率19%。其结构经1H NMR,13C NMR,IR和MS表征。此法绿色环保、成本较低,适合工业化生产。 |
英文摘要: |
The desired compound Sempervilam was prepared from heptanediacid. The total yield of the ten steps is 19%.The structures of all compounds were characterized by 1H NMR, 13C NMR, IR and MS. The method is environmentally friendly, lower cost, and suitable for industrial production. |
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